formula54 (Hive Addict)
12-04-01 17:27
No 244075
      coupling reagent synth  Bookmark   

a synth for O-(7-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate is hinted towards on rhodiums site, anyone got refs for this?
supposed needed chems are oxalyl chloride,
teramethylurea, toluene, ether, chloroform, ammonium hexafluorophosphate(or NH4BF4), DCM, HOBt, and triethylamine.
thanks 54


-swis54
 
 
 
 
    amalgum
(Newbee)
12-04-01 20:59
No 244137
      Re: coupling reagent synth  Bookmark   

Why do you want to make a PCR when you can just buy one?