![]() |
![]() |
|||||||
El_Zorro
(Hive Addict) 12-03-02 07:46 No 385754 |
![]() |
Dimethyl sulfate hell | Bookmark | |||||
Alright, where the hell does a non-professional chemist get DMS?? I guess I could make some MeI, but I don't have LG RP, and I don't feel like getting the HUGE amounts of matchbooks that would be required to make the amount of MeI worthwhile. I've thought about saying fuck it and just running a reaction like the one at Rhodium's site to make diethyl sulfate, just substituting methanol. ../rhodium /diethyl But then, there's also the huge risk of cancer. ![]() It is seductive, way too seductive. -Eleusis |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
moo (Hive Bee) 12-03-02 09:41 No 385776 |
![]() |
Read these first | Bookmark | |||||
For the preparation of dimethyl sulfate (DMS) Post 278794 (halfapint: "Re: Dimethyl/Diethyl Sulfate", Chemistry Discourse) seems to be the easiest synthesis, read the whole thread too. Then there are also Post 208007 (legionbob: "OTC preperation of Dimethyl sulfate?", Tryptamine Chemistry) and Post 55178 (dildoque: "DMS", Chemistry Discourse). I could've said UTFSE but I guess posting links to the good stuff also makes UTFSE easier. |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
Protium (Hive Bee) 12-03-02 09:58 No 385777 |
![]() |
Just to avoid any confusion | Bookmark | |||||
There is a big difference between DMS and DMS. That is, dimethyl sulfide, and dimethyl sulfate. Threw me off for a second reading it until I realized that both share the same acronym. Pr(+)tium |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
Rhodium (Chief Bee) 12-04-02 11:58 No 386143 |
![]() |
Got a fume hood? | Bookmark | |||||
Zorro: If you have a fume hood, then making it yourself is no problem, it has been discussed extensively by Halfapint and Antoncho et al. |
||||||||
![]() |
![]() |
|||||||