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Grignard
03-30-04 12:55 |
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(Rated as: UTFSE!) |
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Rhodium (Chief Bee) 03-30-04 13:46 No 498150 |
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UTFSE! | ||||||
It was too hard to UTFSE, I suppose? The following thread is among the top 20 in this forum even: Post 477883 (Rhodium: "Practical Total Synthesis of Cocaine", Methods Discourse) The Hive - Clandestine Chemists Without Borders |
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Grignard (Hive Bee) 03-30-04 16:44 No 498178 |
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yes a lot of references there, but i dont find | ||||||
yes a lot of references there, but i dont find an answer on how to make Methylecgonine from tropinone.. In this old text they reduce tropinone with raney Ni, Is this a process that will work and under what yield? it is this reference i would like to see... |
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Rhodium (Chief Bee) 03-30-04 17:13 No 498181 |
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did you read the whole thread? | ||||||
The Findlay paper here converts tropinone to 2-carbomethoxytropinone: Post 488336 (Rhodium: "Synthesis of Tropinone & 2-CMT", Methods Discourse) And the links at the bottom of the page concerns the reduction of the latter to methylecgonine. The papers in Post 487702 (Rhodium: "Willstätter's Classic Cocaine Synthesis", Methods Discourse) also details the procedure. The Hive - Clandestine Chemists Without Borders |
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roger2003 (Hive Bee) 03-31-04 05:02 No 498263 |
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cocaine from tropinone | ||||||
See: Patent DE406215 roger2003 |
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