synthetikal.com Forum Index


benzene purification
Page 1 of 1
Post new topic   Reply to topic    synthetikal.com Forum Index -> Essential Methods
Author Message
nubee
Master Archiver
Joined: 18 Feb 2005
Posts: 213
Location: homeless
18579.78 Points

Tue Apr 19, 2005 6:50 am
Reply with quote

Very pure benzene is best prepared from the commercial product by repeatedly shaking it with small quantities of sulphuric acid to remove thiophen, C4 H4 S, which is not easily removed in any other way. The product is fractionated and then partly frozen. The unfrozen liquid retains most of the impurities, and the crystals separating at 5oC. are very pure benzene.
Back to top
TokenJ

Joined: 20 Jun 2005
Posts: 9
274.80 Points

Wed Jul 20, 2005 6:58 pm
Reply with quote

fraction distalation is you best bet. but i have heard of fraction crystaliseation
Back to top
TokenJ

Joined: 20 Jun 2005
Posts: 9
274.80 Points

Wed Jul 20, 2005 6:59 pm
Reply with quote

fraction distalation is you best bet. but i have heard of fraction crystaliseation
Back to top
Display posts from previous:   
Post new topic   Reply to topic    synthetikal.com Forum Index -> Essential Methods All times are GMT + 5.5 Hours
Page 1 of 1

 



Powered by phpBB 2.0.11 © 2001, 2002 phpBB Group

Igloo Theme Version 1.0 :: Created By: Andrew Charron