psychokitty («») 09-16-04 04:49 No 531553 |
N-Halosaccharin for halogenations? (Rated as: add bibliographic data!) |
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In the PDF document listed on this page is information about the preparation of N-chloro- and N-bromosaccharin. Both can be likely be applied to just about any halogenation reaction. A Green Preparation of N-Chloro- and N-Bromosaccharin: |
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java (Hive Addict) 09-16-04 19:33 No 531642 |
N-Halosaccharin for Halogenation (biograph added) | |||||||
Note Re-post intended to assist in making the article posted by psychokitty more appealing to the Bee's A Green Preparation of N-Chloro- and N-Bromosaccharin Soraia P. L. de Souza, Joaquim F. M. da Silva, and Marcio C. S. de Mattos* SYNTHETIC COMMUNICATIONS Vol. 33, No. 6, pp. 935–939, 2003 Full Text:posted pdf by psychokitty......Post 531553 (psychokitty: "N-Halosaccharin for halogenations?", Chemistry Discourse) Abstract The reaction of the sodium salt of saccharin, potassium chloride or bromide and oxone in water at room temperature for 24 h produced pure N-chloro- and N-bromosaccharin in 58% and64% yield, respectively. It is better to die on your feet than to live on your knees....... -Emiliano Zapata- |
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