psychokitty
(«»)
09-16-04 04:49
No 531553
      N-Halosaccharin for halogenations?
(Rated as: add bibliographic data!)
    

In the PDF document listed on this page is information about the preparation of N-chloro- and N-bromosaccharin.  Both can be likely be applied to just about any halogenation reaction.

A Green Preparation of N-Chloro- and N-Bromosaccharin:

 
 
 
 
    java
(Hive Addict)
09-16-04 19:33
No 531642
      N-Halosaccharin for Halogenation (biograph added)     

Note Re-post intended to assist in making the article posted by psychokitty more appealing to the Bee's

A Green Preparation of N-Chloro- and N-Bromosaccharin

Soraia P. L. de Souza, Joaquim F. M. da Silva, and Marcio C. S. de Mattos*

SYNTHETIC COMMUNICATIONS  Vol. 33, No. 6, pp. 935–939, 2003

Full Text:posted pdf by psychokitty......Post 531553 (psychokitty: "N-Halosaccharin for halogenations?", Chemistry Discourse)

Abstract The reaction of the sodium salt of saccharin, potassium chloride or bromide and oxone  in water at room temperature for 24 h produced pure N-chloro- and N-bromosaccharin in 58% and64% yield, respectively.

It is better to die on your feet than to live on your knees.......
-Emiliano Zapata-