n00dle
(Stranger) 08-17-03 05:31 No 454018 |
DMT synth with alternate reducing agent | |||||||
Hi. Please forgive the noobness :) I was just reading ../rhodium /dmtsyn. |
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Bandil (Hive Bee) 08-17-03 11:24 No 454079 |
Yes, but AFAIK that method only yeilds about... | |||||||
Yes, but AFAIK that method only yeilds about 20% tops.... Size doesn't matter, it's the sound you make when hitting the ground after smoking it, that matters! |
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n00dle (Stranger) 08-17-03 13:05 No 454091 |
ouchies. are there any other options? | |||||||
ouchies. are there any other options? assuming sodium cyanoborohydride is watched heavily. |
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Bandil (Hive Bee) 08-17-03 14:04 No 454096 |
Sodium borohydride can also be used, and gives | |||||||
Sodium borohydride can also be used, and gives high yeilds... Size doesn't matter, it's the sound you make when hitting the ground after smoking it, that matters! |
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Rhodium (Chief Bee) 08-17-03 14:15 No 454097 |
Clarification | |||||||
Using slow concurrent addition of NaBH4 and formaldehyde at low temp, though. A recent post in this forum explains the special techniques needed when using borohydride instead of cyanoborohydride: Post 436291 (Lego: "What am I not seeing here?", Tryptamine Chemistry) |
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Noid (Hive Bee) 08-18-03 06:27 No 454281 |
fellow explorers wanted: | |||||||
You can also start from indole, as posted here Post 451545 (Chimimanie: "Thanks", Tryptamine Chemistry) The Indolyl-3-dimethylaminomethylketone gets reduced to DMT via NaBH4 in 1-propanol. I read it may be possible to use another solvent, but no one backed up that thought so maybe not. If you can get SnCl4 (anhdrous liquid) and NaBH4 than your good to go. The rest is non sketch and easily obtainable. 48% |
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